IndiumV3, Main, Repository, bibRecord, 002329

The effect of linker of electrodes prepared from sol-gel ionic liquid precursor and carbon nanoparticles on dioxygen electroreduction bioelectrocatalysis

Identifieur interne : 002329 ( Main/Repository ); précédent : 002328; suivant : 002330

The effect of linker of electrodes prepared from sol-gel ionic liquid precursor and carbon nanoparticles on dioxygen electroreduction bioelectrocatalysis

Auteurs : RBID : Pascal:12-0336249

Descripteurs français

Pascal (Inist)
- Electrode ITO, Préparation, Procédé sol gel, Liquide ionique, Précurseur, Carbone, Nanoparticule, Oxygène, Réduction chimique, Catalyse enzymatique, Enzyme immobilisée, Electrocatalyse, Couche multimoléculaire mixte, Couche autoassemblée, Silicate organique, Autoassemblage, Bioélectrochimie, Bilirubin oxidase, Cinétique, Voltammétrie cyclique, Réaction électrochimique, Imidazolium(1-méthyl-3-[3-(triméthoxysilyl)propyl]) amidure(bis[trifluoromésyl]), Silane(tétraméthoxy), 2,2p-Azinobis[benzothiazoline-6-sulfonique acide](3,3p-diéthyl).
Wicri :
- concept : Carbone, Oxygène.

English descriptors

KwdEn :
- Bilirubin oxidase, Bioelectrochemistry, Carbon, Chemical reduction, Cyclic voltammetry, Electrocatalysis, Electrochemical reaction, Enzymatic catalysis, Immobilized enzyme, Indium tin oxide electrode, Ionic liquid, Kinetics, Mixed multilayer, Nanoparticle, Organic silicate, Oxygen, Precursor, Preparation, Self assembly, Self-assembled layer, Sol gel process.

Abstract

The effect of linker of three-dimensional, hydrophilic-carbon-nanoparticle film-electrodes prepared by layer-by-layer method on redox probe accumulation and bioelectrocatalytic dioxygen reduction was studied and compared for two different electrode scaffolds. The linker in both of these scaffolds was based on the same ionic liquid sol-gel precursor, 1-methyl-3-(3-trimethoxysilylpropyl) imidazolium bis(trifluoromethyl-sulfonyl)imide. The first electrode type was prepared by alternative immersion of tin doped indium oxide substrate in an aqueous suspension of carbon nanoparticles modified with phenyl sulphonic groups and a sol composed of ionic liquid sol-gel precursor and tetramethoxysilane. For the second electrode type sol was replaced by a methanolic suspension of silicate submicroparticles with appended imidazolium functional groups. In both films 2,2'-azino-bis(3-ethylbenzothiazoline-6-sulfonate) anions accumulate irreversibly. In the case of the first electrode electrostatic attraction plays the more important role in comparison to the case of the second where stable adsorption of the redox probe takes place. After adsorption of bilirubin oxidase, electrodes obtained from sol and carbon nanoparticles exhibit modest bioelectrocatalytic activity towards dioxygen reduction at pH 4.8, however those obtained from oppositely charged particles are much more efficient. The magnitude of the associated catalytic current in both cases depends on the number of immersion and withdrawal steps. Interestingly, mediatorless catalysis at electrodes obtained from oppositely charged particles is more efficient than mediated catalysis.

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Pascal:12-0336249

Le document en format XML

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<author><name sortKey="Gaillon, Laurent" uniqKey="Gaillon L">Laurent Gaillon</name>
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<author><name sortKey="Opallo, Marcin" uniqKey="Opallo M">Marcin Opallo</name>
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<title level="j" type="abbreviated">Electrochim. acta</title>
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<profileDesc><textClass><keywords scheme="KwdEn" xml:lang="en"><term>Bilirubin oxidase</term>
<term>Bioelectrochemistry</term>
<term>Carbon</term>
<term>Chemical reduction</term>
<term>Cyclic voltammetry</term>
<term>Electrocatalysis</term>
<term>Electrochemical reaction</term>
<term>Enzymatic catalysis</term>
<term>Immobilized enzyme</term>
<term>Indium tin oxide electrode</term>
<term>Ionic liquid</term>
<term>Kinetics</term>
<term>Mixed multilayer</term>
<term>Nanoparticle</term>
<term>Organic silicate</term>
<term>Oxygen</term>
<term>Precursor</term>
<term>Preparation</term>
<term>Self assembly</term>
<term>Self-assembled layer</term>
<term>Sol gel process</term>
</keywords>
<keywords scheme="Pascal" xml:lang="fr"><term>Electrode ITO</term>
<term>Préparation</term>
<term>Procédé sol gel</term>
<term>Liquide ionique</term>
<term>Précurseur</term>
<term>Carbone</term>
<term>Nanoparticule</term>
<term>Oxygène</term>
<term>Réduction chimique</term>
<term>Catalyse enzymatique</term>
<term>Enzyme immobilisée</term>
<term>Electrocatalyse</term>
<term>Couche multimoléculaire mixte</term>
<term>Couche autoassemblée</term>
<term>Silicate organique</term>
<term>Autoassemblage</term>
<term>Bioélectrochimie</term>
<term>Bilirubin oxidase</term>
<term>Cinétique</term>
<term>Voltammétrie cyclique</term>
<term>Réaction électrochimique</term>
<term>Imidazolium(1-méthyl-3-[3-(triméthoxysilyl)propyl]) amidure(bis[trifluoromésyl])</term>
<term>Silane(tétraméthoxy)</term>
<term>2,2p-Azinobis[benzothiazoline-6-sulfonique acide](3,3p-diéthyl)</term>
</keywords>
<keywords scheme="Wicri" type="concept" xml:lang="fr"><term>Carbone</term>
<term>Oxygène</term>
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<front><div type="abstract" xml:lang="en">The effect of linker of three-dimensional, hydrophilic-carbon-nanoparticle film-electrodes prepared by layer-by-layer method on redox probe accumulation and bioelectrocatalytic dioxygen reduction was studied and compared for two different electrode scaffolds. The linker in both of these scaffolds was based on the same ionic liquid sol-gel precursor, 1-methyl-3-(3-trimethoxysilylpropyl) imidazolium bis(trifluoromethyl-sulfonyl)imide. The first electrode type was prepared by alternative immersion of tin doped indium oxide substrate in an aqueous suspension of carbon nanoparticles modified with phenyl sulphonic groups and a sol composed of ionic liquid sol-gel precursor and tetramethoxysilane. For the second electrode type sol was replaced by a methanolic suspension of silicate submicroparticles with appended imidazolium functional groups. In both films 2,2'-azino-bis(3-ethylbenzothiazoline-6-sulfonate) anions accumulate irreversibly. In the case of the first electrode electrostatic attraction plays the more important role in comparison to the case of the second where stable adsorption of the redox probe takes place. After adsorption of bilirubin oxidase, electrodes obtained from sol and carbon nanoparticles exhibit modest bioelectrocatalytic activity towards dioxygen reduction at pH 4.8, however those obtained from oppositely charged particles are much more efficient. The magnitude of the associated catalytic current in both cases depends on the number of immersion and withdrawal steps. Interestingly, mediatorless catalysis at electrodes obtained from oppositely charged particles is more efficient than mediated catalysis.</div>
</front>
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<fA08 i1="01" i2="1" l="ENG"><s1>The effect of linker of electrodes prepared from sol-gel ionic liquid precursor and carbon nanoparticles on dioxygen electroreduction bioelectrocatalysis</s1>
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</fC03>
<fC03 i1="05" i2="X" l="SPA"><s0>Precursor</s0>
<s5>05</s5>
</fC03>
<fC03 i1="06" i2="X" l="FRE"><s0>Carbone</s0>
<s2>NC</s2>
<s5>06</s5>
</fC03>
<fC03 i1="06" i2="X" l="ENG"><s0>Carbon</s0>
<s2>NC</s2>
<s5>06</s5>
</fC03>
<fC03 i1="06" i2="X" l="SPA"><s0>Carbono</s0>
<s2>NC</s2>
<s5>06</s5>
</fC03>
<fC03 i1="07" i2="X" l="FRE"><s0>Nanoparticule</s0>
<s5>07</s5>
</fC03>
<fC03 i1="07" i2="X" l="ENG"><s0>Nanoparticle</s0>
<s5>07</s5>
</fC03>
<fC03 i1="07" i2="X" l="SPA"><s0>Nanopartícula</s0>
<s5>07</s5>
</fC03>
<fC03 i1="08" i2="X" l="FRE"><s0>Oxygène</s0>
<s2>NC</s2>
<s2>FX</s2>
<s5>08</s5>
</fC03>
<fC03 i1="08" i2="X" l="ENG"><s0>Oxygen</s0>
<s2>NC</s2>
<s2>FX</s2>
<s5>08</s5>
</fC03>
<fC03 i1="08" i2="X" l="SPA"><s0>Oxígeno</s0>
<s2>NC</s2>
<s2>FX</s2>
<s5>08</s5>
</fC03>
<fC03 i1="09" i2="X" l="FRE"><s0>Réduction chimique</s0>
<s5>09</s5>
</fC03>
<fC03 i1="09" i2="X" l="ENG"><s0>Chemical reduction</s0>
<s5>09</s5>
</fC03>
<fC03 i1="09" i2="X" l="SPA"><s0>Reducción química</s0>
<s5>09</s5>
</fC03>
<fC03 i1="10" i2="X" l="FRE"><s0>Catalyse enzymatique</s0>
<s5>10</s5>
</fC03>
<fC03 i1="10" i2="X" l="ENG"><s0>Enzymatic catalysis</s0>
<s5>10</s5>
</fC03>
<fC03 i1="10" i2="X" l="SPA"><s0>Catálisis enzimática</s0>
<s5>10</s5>
</fC03>
<fC03 i1="11" i2="X" l="FRE"><s0>Enzyme immobilisée</s0>
<s5>11</s5>
</fC03>
<fC03 i1="11" i2="X" l="ENG"><s0>Immobilized enzyme</s0>
<s5>11</s5>
</fC03>
<fC03 i1="11" i2="X" l="SPA"><s0>Enzima inmovilizada</s0>
<s5>11</s5>
</fC03>
<fC03 i1="12" i2="X" l="FRE"><s0>Electrocatalyse</s0>
<s5>12</s5>
</fC03>
<fC03 i1="12" i2="X" l="ENG"><s0>Electrocatalysis</s0>
<s5>12</s5>
</fC03>
<fC03 i1="12" i2="X" l="SPA"><s0>Electrocatálisis</s0>
<s5>12</s5>
</fC03>
<fC03 i1="13" i2="X" l="FRE"><s0>Couche multimoléculaire mixte</s0>
<s5>13</s5>
</fC03>
<fC03 i1="13" i2="X" l="ENG"><s0>Mixed multilayer</s0>
<s5>13</s5>
</fC03>
<fC03 i1="13" i2="X" l="SPA"><s0>Capa multimolecular mixta</s0>
<s5>13</s5>
</fC03>
<fC03 i1="14" i2="X" l="FRE"><s0>Couche autoassemblée</s0>
<s5>14</s5>
</fC03>
<fC03 i1="14" i2="X" l="ENG"><s0>Self-assembled layer</s0>
<s5>14</s5>
</fC03>
<fC03 i1="14" i2="X" l="SPA"><s0>Capa autoensamblada</s0>
<s5>14</s5>
</fC03>
<fC03 i1="15" i2="X" l="FRE"><s0>Silicate organique</s0>
<s5>15</s5>
</fC03>
<fC03 i1="15" i2="X" l="ENG"><s0>Organic silicate</s0>
<s5>15</s5>
</fC03>
<fC03 i1="15" i2="X" l="SPA"><s0>Silicato orgánico</s0>
<s5>15</s5>
</fC03>
<fC03 i1="16" i2="X" l="FRE"><s0>Autoassemblage</s0>
<s5>16</s5>
</fC03>
<fC03 i1="16" i2="X" l="ENG"><s0>Self assembly</s0>
<s5>16</s5>
</fC03>
<fC03 i1="16" i2="X" l="SPA"><s0>Autoensamble</s0>
<s5>16</s5>
</fC03>
<fC03 i1="17" i2="X" l="FRE"><s0>Bioélectrochimie</s0>
<s5>17</s5>
</fC03>
<fC03 i1="17" i2="X" l="ENG"><s0>Bioelectrochemistry</s0>
<s5>17</s5>
</fC03>
<fC03 i1="17" i2="X" l="SPA"><s0>Bioelectroquímica</s0>
<s5>17</s5>
</fC03>
<fC03 i1="18" i2="X" l="FRE"><s0>Bilirubin oxidase</s0>
<s2>FE</s2>
<s5>18</s5>
</fC03>
<fC03 i1="18" i2="X" l="ENG"><s0>Bilirubin oxidase</s0>
<s2>FE</s2>
<s5>18</s5>
</fC03>
<fC03 i1="18" i2="X" l="SPA"><s0>Bilirubin oxidase</s0>
<s2>FE</s2>
<s5>18</s5>
</fC03>
<fC03 i1="19" i2="X" l="FRE"><s0>Cinétique</s0>
<s5>19</s5>
</fC03>
<fC03 i1="19" i2="X" l="ENG"><s0>Kinetics</s0>
<s5>19</s5>
</fC03>
<fC03 i1="19" i2="X" l="SPA"><s0>Cinética</s0>
<s5>19</s5>
</fC03>
<fC03 i1="20" i2="X" l="FRE"><s0>Voltammétrie cyclique</s0>
<s5>20</s5>
</fC03>
<fC03 i1="20" i2="X" l="ENG"><s0>Cyclic voltammetry</s0>
<s5>20</s5>
</fC03>
<fC03 i1="20" i2="X" l="SPA"><s0>Voltametría cíclica</s0>
<s5>20</s5>
</fC03>
<fC03 i1="21" i2="X" l="FRE"><s0>Réaction électrochimique</s0>
<s5>32</s5>
</fC03>
<fC03 i1="21" i2="X" l="ENG"><s0>Electrochemical reaction</s0>
<s5>32</s5>
</fC03>
<fC03 i1="21" i2="X" l="SPA"><s0>Reacción electroquímica</s0>
<s5>32</s5>
</fC03>
<fC03 i1="22" i2="X" l="FRE"><s0>Imidazolium(1-méthyl-3-[3-(triméthoxysilyl)propyl]) amidure(bis[trifluoromésyl])</s0>
<s2>NK</s2>
<s4>INC</s4>
<s5>76</s5>
</fC03>
<fC03 i1="23" i2="X" l="FRE"><s0>Silane(tétraméthoxy)</s0>
<s2>NK</s2>
<s4>INC</s4>
<s5>77</s5>
</fC03>
<fC03 i1="24" i2="X" l="FRE"><s0>2,2p-Azinobis[benzothiazoline-6-sulfonique acide](3,3p-diéthyl)</s0>
<s2>NK</s2>
<s4>INC</s4>
<s5>78</s5>
</fC03>
<fC07 i1="01" i2="X" l="FRE"><s0>Oxidoreductases</s0>
<s2>FE</s2>
</fC07>
<fC07 i1="01" i2="X" l="ENG"><s0>Oxidoreductases</s0>
<s2>FE</s2>
</fC07>
<fC07 i1="01" i2="X" l="SPA"><s0>Oxidoreductases</s0>
<s2>FE</s2>
</fC07>
<fC07 i1="02" i2="X" l="FRE"><s0>Enzyme</s0>
<s2>FE</s2>
</fC07>
<fC07 i1="02" i2="X" l="ENG"><s0>Enzyme</s0>
<s2>FE</s2>
</fC07>
<fC07 i1="02" i2="X" l="SPA"><s0>Enzima</s0>
<s2>FE</s2>
</fC07>
<fN21><s1>254</s1>
</fN21>
</pA>
<pR><fA30 i1="01" i2="1" l="ENG"><s1>International Society of Electrochemistry (ISE) Meeting</s1>
<s2>61</s2>
<s3>Nice FRA</s3>
<s4>2010-09-26</s4>
</fA30>
</pR>
</standard>
</inist>
</record>

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The effect of linker of electrodes prepared from sol-gel ionic liquid precursor and carbon nanoparticles on dioxygen electroreduction bioelectrocatalysis

The effect of linker of electrodes prepared from sol-gel ionic liquid precursor and carbon nanoparticles on dioxygen electroreduction bioelectrocatalysis

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